ASTM E1858 – Standard Test Methods for Determining Oxidation Induction Time of Hydrocarbons by Differential Scanning Calorimetry
Significance and Use
5.1Â Oxidative induction time is a relative measure of the degree of oxidative stability of the material evaluated at the isothermal temperature of the test. The presence, quantity or effectiveness of antioxidants may be determined by this method. The OIT values thus obtained may be compared from one hydrocarbon to another or to a reference material to obtain relative oxidative stability information.
5.2Â Typical uses include the oxidative stability of edible oils and fats (oxidative rancidity), lubricants, greases, and polyolefins.
Scope
1.1Â These test methods describe the determination of the oxidative properties of hydrocarbons by differential scanning calorimetry or pressure differential scanning calorimetry and is applicable to hydrocarbons that oxidize exothermically in their analyzed form.
1.2 Test Method A—A differential scanning calorimeter (DSC) is used at ambient pressure, for example, about 100 kPa of oxygen.
1.3 Test Method B—A pressure DSC (PDSC) is used at high pressure, for example, 3.5 MPa (500 psig) oxygen.
1.4 Units—The values stated in SI units are to be regarded as standard. Imperial units are provided for user convenience and are not the standard.
1.5 These test methods are related to ISO 11357–6 but is different in technical content. These test methods are related to CEC L-85–T but includes additional experimental conditions.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 7.4 and 12.10.
1.7Â This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Extracted, with permission, from ASTM E1858 – Standard Test Methods for Determining Oxidation Induction Time of Hydrocarbons by Differential Scanning Calorimetry, copyright ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428. A copy of the complete standard may be purchased from ASTM International, astm.org
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